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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="en"><front><journal-meta><journal-id journal-id-type="publisher-id">najo</journal-id><journal-title-group><journal-title xml:lang="en">Nanosystems: Physics, Chemistry, Mathematics</journal-title><trans-title-group xml:lang="ru"><trans-title>Наносистемы: физика, химия, математика</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">2220-8054</issn><issn pub-type="epub">2305-7971</issn><publisher><publisher-name>Университет ИТМО</publisher-name></publisher></journal-meta><article-meta><article-id custom-type="elpub" pub-id-type="custom">najo-1088</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>CHEMISTRY AND MATERIALS SCIENCE</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ХИМИЯ И НАУКА О МАТЕРИАЛАХ</subject></subj-group></article-categories><title-group><article-title>Effect of hydrothermal synthesis conditions on the morphology of ZrO2 nanoparticles</article-title><trans-title-group xml:lang="ru"><trans-title></trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Bugrov</surname><given-names>A. N.</given-names></name></name-alternatives><bio xml:lang="en"><p>Saint Petersburg.</p></bio><email xlink:type="simple">bugrov.an@mail.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Almjasheva</surname><given-names>O. V.</given-names></name></name-alternatives><bio xml:lang="en"><p>Saint Petersburg.</p></bio><email xlink:type="simple">almjasheva@mail.ru</email><xref ref-type="aff" rid="aff-2"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="en">Institute of Macromolecular Compounds RAS; Saint Petersburg Electrotechnical University “LETI”<country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="en">Saint Petersburg Electrotechnical University “LETI”; Ioffe Physical-Technical Institute RAS<country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2013</year></pub-date><pub-date pub-type="epub"><day>17</day><month>08</month><year>2025</year></pub-date><volume>4</volume><issue>6</issue><fpage>810</fpage><lpage>815</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Bugrov A.N., Almjasheva O.V., 2025</copyright-statement><copyright-year>2025</copyright-year><copyright-holder xml:lang="ru">Bugrov A.N., Almjasheva O.V.</copyright-holder><copyright-holder xml:lang="en">Bugrov A.N., Almjasheva O.V.</copyright-holder><license license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://nanojournal.ifmo.ru/jour/article/view/1088">https://nanojournal.ifmo.ru/jour/article/view/1088</self-uri><abstract><p>Nanoparticles based on ZrO2 in the form of spheres, cylinders and agglomerates in the form of hollow microspheres were obtained. It is shown that the main factor influencing on the formation of nanostructures based on zirconium dioxide under hydrothermal conditions is the chemical prehistory of the starting materials. The possibility of varying the synthetic parameters to obtain a zirconia-based material with high porosity and specific surface area was shown.</p></abstract><kwd-group xml:lang="en"><kwd>nanoparticles</kwd><kwd>hydrothermal synthesis</kwd><kwd>zirconia</kwd></kwd-group><funding-group xml:lang="en"><funding-statement>We are deeply grateful to V.V. Gusarov for the attention to work. This work was supported by the Russian Foundation for Basic Research (grant 13-08-01207).</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">J.P. Jolivet, S. Cassaignon, C. Chan´eac, et al. 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