najoNanosystems: Physics, Chemistry, MathematicsНаносистемы: физика, химия, математика2220-80542305-7971Университет ИТМО10.17586/2220-8054-2016-7-3-459-463najo-1232Research ArticleCHEMISTRY AND MATERIALS SCIENCEХИМИЯ И НАУКА О МАТЕРИАЛАХThe characterization of nanosized ZnFe2O4 material prepared by coprecipitationThe characterization of nanosized ZnFe2O4 material prepared by coprecipitationNguyenА. T.NguyenA. T.

Ho Chi Minh City

Ho Chi Minh City

anhtien0601@rambler.ruPhanPh. H. Nh.PhanPh. H. Nh.

Ho Chi Minh City

Ho Chi Minh City

pphoainhan@gmail.comMittovaI. Ya.MittovaI. Ya.

Voronezh

Voronezh

imittova@mail.ruKnurovaМ. V.KnurovaM. V.

Voronezh

Voronezh

cnurova2010@yandex.ruMittovaV. O.MittovaV. O.

Voronezh

Voronezh

vmittova@mail.ruHo Chi Minh City Pedagogical UniversityHo Chi Minh City Pedagogical UniversityVoronezh State UniversityVoronezh State UniversityVoronezh State Medical University named after N.N. BurdenkoVoronezh State Medical University named after N.N. Burdenko20162008202573459463Copyright © Nguyen A.T., Phan P., Mittova I.Y., Knurova M.V., Mittova V.O., 20252025Nguyen А.T., Phan P., Mittova I.Y., Knurova М.V., Mittova V.O.Nguyen A.T., Phan P., Mittova I.Y., Knurova M.V., Mittova V.O.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://nanojournal.ifmo.ru/jour/article/view/1232

The nanosized ZnFe2O4 material was synthesized using the coprecipitation method from Zn2+ and Fe3+ cations in a boiling aqueous medium. The results of TG/DSC, XRD, SEM, TEM and VSM analysis show that the ZnFe2O4 material prepared after annealing at 600 ◦C had tetragonal structure, a size of 20 – 50 nm, Hc < 70 Oe, Mr < 0.5 emu/g and Ms ∼ 2.5 emu/g.

The nanosized ZnFe2O4 material was synthesized using the coprecipitation method from Zn2+ and Fe3+ cations in a boiling aqueous medium. The results of TG/DSC, XRD, SEM, TEM and VSM analysis show that the ZnFe2O4 material prepared after annealing at 600 ◦C had tetragonal structure, a size of 20 – 50 nm, Hc < 70 Oe, Mr < 0.5 emu/g and Ms ∼ 2.5 emu/g.

sol-gel synthesisnanopowderszinc ferritemagnetic propertiessol-gel synthesisnanopowderszinc ferritemagnetic propertiesThis work was supported by the Ministry of Education and Science of the Russian Federation in line with government order for Higher Education Institutions in the field of science for the years 2014 – 2016 (project No. 225)This work was supported by the Ministry of Education and Science of the Russian Federation in line with government order for Higher Education Institutions in the field of science for the years 2014 – 2016 (project No. 225)ReferencesLuu T.T. Magnetic Materials Lecture. Hanoi National University Publication, 2008, 273 p.Luu T.T. Magnetic Materials Lecture. Hanoi National University Publication, 2008, 273 p.Brusensov Yu.A., Minaev A.M. Fundamentals of physics and technology of oxide semiconductors. Publisher TSTU, Tambov, 2001, 40 p.Brusensov Yu.A., Minaev A.M. Fundamentals of physics and technology of oxide semiconductors. Publisher TSTU, Tambov, 2001, 40 p.Al Angari Y.M. Magnetic properties of La-substituted NiFe2O4 via egg-white precursor route. Journal of Magnetism and Magnetic Materials, 2011, 323, P. 1835–1839.Al Angari Y.M. Magnetic properties of La-substituted NiFe2O4 via egg-white precursor route. Journal of Magnetism and Magnetic Materials, 2011, 323, P. 1835–1839.Kuznetsova V.A., Almjasheva O.V., Gusarov V.V. Influence of microwave and ultrasonic treatment on the formation of CoFe2O4 under hydrothermal conditions. Glass Physics and Chemistry, 2009, 35(2), P. 205–209.Kuznetsova V.A., Almjasheva O.V., Gusarov V.V. Influence of microwave and ultrasonic treatment on the formation of CoFe2O4 under hydrothermal conditions. Glass Physics and Chemistry, 2009, 35(2), P. 205–209.Komlev A.A., Semenova A.S. Magnetic Characteristics of MgFe2O4-containing nanopowders prepared by the hydrothermal method. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(6), P. 105–111. (In Russian)Komlev A.A., Semenova A.S. Magnetic Characteristics of MgFe2O4-containing nanopowders prepared by the hydrothermal method. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(6), P. 105–111. (In Russian)Komlev A.A., Ilhan S. Formation of iron-magnesium spinel nanoparticles under dehydration of co-precipitated magnesium and iron hydroxides. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(4), P. 114–121. (In Russian)Komlev A.A., Ilhan S. Formation of iron-magnesium spinel nanoparticles under dehydration of co-precipitated magnesium and iron hydroxides. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(4), P. 114–121. (In Russian)Luu M.D., Nguyen Th.T.L. Synthesis nanosized CoFe2O4 by gel combustion. Vietnam Chemistry Journal, 2010, 48(4), P. 404–408.Luu M.D., Nguyen Th.T.L. Synthesis nanosized CoFe2O4 by gel combustion. Vietnam Chemistry Journal, 2010, 48(4), P. 404–408.Nguyen Th.T.L., Pham Th.H. Synthesis nanosized ZnMn2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(2), P. 174–179.Nguyen Th.T.L., Pham Th.H. Synthesis nanosized ZnMn2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(2), P. 174–179.Nguyen A.T., Mittova I.Ya., et al. Influence of the preparation condition on the size and morphology of nanocrystalline lanthanum orthoferrite. Glass Physics and Chemistry, 2008, 34(6), P. 756–761.Nguyen A.T., Mittova I.Ya., et al. Influence of the preparation condition on the size and morphology of nanocrystalline lanthanum orthoferrite. Glass Physics and Chemistry, 2008, 34(6), P. 756–761.Nguyen A.T., Mittova I.Ya., Almjasheva O.V. Influence of the synthesis conditions on the particle size and morphology of yttrium orthoferrite obtained from aqueous solutions. Russian Journal of Applied Chemistry, 2009, 82(11), P. 1915–1918.Nguyen A.T., Mittova I.Ya., Almjasheva O.V. Influence of the synthesis conditions on the particle size and morphology of yttrium orthoferrite obtained from aqueous solutions. Russian Journal of Applied Chemistry, 2009, 82(11), P. 1915–1918.Nguyen Th.T.L. Synthesis nanosized ZnFe2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(3), P. 312–316.Nguyen Th.T.L. Synthesis nanosized ZnFe2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(3), P. 312–316.Nazarenko V.A., Antonovich V.P., Nevskaya E.M. Metal ions hydrolysis in dilute solutions. Atomizdat, Moscow, 1979, 192 p.Nazarenko V.A., Antonovich V.P., Nevskaya E.M. Metal ions hydrolysis in dilute solutions. Atomizdat, Moscow, 1979, 192 p.

The authors declare that there are no conflicts of interest present.