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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="en"><front><journal-meta><journal-id journal-id-type="publisher-id">najo</journal-id><journal-title-group><journal-title xml:lang="en">Nanosystems: Physics, Chemistry, Mathematics</journal-title><trans-title-group xml:lang="ru"><trans-title>Наносистемы: физика, химия, математика</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">2220-8054</issn><issn pub-type="epub">2305-7971</issn><publisher><publisher-name>Университет ИТМО</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.17586/2220-8054-2023-14-3-363-371</article-id><article-id custom-type="elpub" pub-id-type="custom">najo-328</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>CHEMISTRY AND MATERIALS SCIENCE</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ХИМИЯ И НАУКА О МАТЕРИАЛАХ</subject></subj-group></article-categories><title-group><article-title>Influence of the composition of the BiPO4–BiVO4 system on the phase formation, morphology, and properties of nanocrystalline composites obtained under hydrothermal conditions</article-title><trans-title-group xml:lang="ru"><trans-title>Влияние состава системы BiPO4-BiVO4 на фазообразование, морфологию и свойства нанокристаллических композитов, полученных в гидротермальных условиях</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0002-2807-375X</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Проскурина</surname><given-names>О. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Proskurina</surname><given-names>O. V.</given-names></name></name-alternatives><bio xml:lang="en"><p>Olga V. Proskurina</p><p>194021 St. Petersburg</p><p>190013 St. Petersburg</p></bio><email xlink:type="simple">proskurinaov@mail.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0009-0008-7287-298X</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Четинел</surname><given-names>И. Д.</given-names></name><name name-style="western" xml:lang="en"><surname>Chetinel</surname><given-names>I. D.</given-names></name></name-alternatives><bio xml:lang="en"><p>Ilke Diana Chetine</p><p>190013 St. Petersburg</p></bio><email xlink:type="simple">diana03ridak@gmail.com</email><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0002-3304-9068</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Сероглазова</surname><given-names>А. С.</given-names></name><name name-style="western" xml:lang="en"><surname>Seroglazova</surname><given-names>A. S.</given-names></name></name-alternatives><bio xml:lang="en"><p>Anna S. Seroglazova</p><p>194021 St. Petersburg</p><p>190013 St. Petersburg</p></bio><email xlink:type="simple">annaseroglazova@yandex.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0003-4375-6388</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Гусаров</surname><given-names>В. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Gusarov</surname><given-names>V. V.</given-names></name></name-alternatives><bio xml:lang="en"><p>Victor V. Gusarov</p><p>194021 St. Petersburg</p></bio><email xlink:type="simple">victor.v.gusarov@gmail.com</email><xref ref-type="aff" rid="aff-3"/></contrib></contrib-group><aff xml:lang="en" id="aff-1"><institution>Ioffe Institute; St. Petersburg State Institute of Technology</institution><country>Russian Federation</country></aff><aff xml:lang="en" id="aff-2"><institution>St. Petersburg State Institute of Technology</institution><country>Russian Federation</country></aff><aff xml:lang="en" id="aff-3"><institution>Ioffe Institute</institution><country>Russian Federation</country></aff><pub-date pub-type="collection"><year>2023</year></pub-date><pub-date pub-type="epub"><day>30</day><month>06</month><year>2025</year></pub-date><volume>14</volume><issue>3</issue><fpage>363</fpage><lpage>371</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Proskurina O.V., Chetinel I.D., Seroglazova A.S., Gusarov V.V., 2025</copyright-statement><copyright-year>2025</copyright-year><copyright-holder xml:lang="ru">Проскурина О.В., Четинел И.Д., Сероглазова А.С., Гусаров В.В.</copyright-holder><copyright-holder xml:lang="en">Proskurina O.V., Chetinel I.D., Seroglazova A.S., Gusarov V.V.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://nanojournal.ifmo.ru/jour/article/view/328">https://nanojournal.ifmo.ru/jour/article/view/328</self-uri><abstract><p>BiPO4/BiVO4 nanocrystalline composites were synthesized under hydrothermal conditions. The influence of the initial composition of the system on the phase state, the size of crystallites, and the morphology of the formed particles was determined. The photocatalytic activity of the nanocomposite was studied using the decomposition of methyl violet as an example.</p></abstract><trans-abstract xml:lang="ru"><p>Нанокристаллические композиты BiPO4/BiVO4 синтезированы в гидротермальных условиях. Определено влияние исходного состава системы на фазовое состояние, размер кристаллитов и морфологию образующихся частиц. На примере разложения метилового фиолетового изучена фотокаталитическая активность нанокомпозита.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>гидротермальный синтез</kwd><kwd>фазообразование</kwd><kwd>нанокристаллы</kwd><kwd>ортофосфат висмута</kwd><kwd>ортованадат висмута</kwd></kwd-group><kwd-group xml:lang="en"><kwd>hydrothermal synthesis</kwd><kwd>phase formation</kwd><kwd>nanocrystals</kwd><kwd>bismuth orthophosphate</kwd><kwd>bismuth orthovanadate</kwd></kwd-group><funding-group><funding-statement xml:lang="en">X-ray diffraction studies were performed employing the equipment of the Engineering Center of the St. Petersburg State Institute of Technology. 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