najoNanosystems: Physics, Chemistry, MathematicsНаносистемы: физика, химия, математика2220-80542305-7971Университет ИТМО10.17586/2220-8054-2017-8-3-378-381najo-615Research ArticlePHYSICSФИЗИКАThe microstructure of the surface of thin PbS films deposited from the coordination compounds diacetatodi(thiourea)leadSemenovV. N.

Universitetskaya sq., 1, Voronezh 394018

NitutaA. N.

Universitetskaya sq., 1, Voronezh 394018

asiyat.nituta@yandex.ruLukinA. N.

Universitetskaya sq., 1, Voronezh 394018

OvechkinaN. M.

Universitetskaya sq., 1, Voronezh 394018

NikitinL. N.

Universitetskaya sq., 1, Voronezh 394018

Voronezh State UniversityRussian Federation20171108202583378381Copyright © Semenov V.N., Nituta A.N., Lukin A.N., Ovechkina N.M., Nikitin L.N., 20252025Semenov V.N., Nituta A.N., Lukin A.N., Ovechkina N.M., Nikitin L.N.Semenov V.N., Nituta A.N., Lukin A.N., Ovechkina N.M., Nikitin L.N.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://nanojournal.ifmo.ru/jour/article/view/615

This paper presents the results from a study of the microstructure of the surface of lead sulfide films deposited via the pyrolysis of aqueous [Pb(N2H4CS)2(CH3COO)2] aerosols. The influences of temperature and the concentration of thiourea on the synthesized films’ surface topography were investigated. A change in the type of conductivity with increasing temperature was observed.

method of aerosol pyrolysispyrolytic filmscoordination compoundssurface microstructuretype of conductivityThe authors wish to thank the Center for Collective Use of Voronezh State University for providing analytical equipment.ReferencesKaupp G. Atomic force microscopy, scanning nearfield optical microscopy and nanoscratching. Application to rough and natural surfaces. Springer-Verlag, Berlin Heidelberg, 2006, 296 p.Kaupp G. Atomic force microscopy, scanning nearfield optical microscopy and nanoscratching. Application to rough and natural surfaces. Springer-Verlag, Berlin Heidelberg, 2006, 296 p.Almjasheva O.V. Formation and structural transformations of nanoparticles in the TiO2–H2O system. Nanosystems: physics, chemistry, mathematics, 2016, 7(6), P. 1031–1049.Almjasheva O.V. Formation and structural transformations of nanoparticles in the TiO2–H2O system. Nanosystems: physics, chemistry, mathematics, 2016, 7(6), P. 1031–1049.Nguyen A.T., Phan Ph.H.Nh.,Mittova I.Ya., Knurova M.V., Mittova V.O. The characterization of nanosized ZnFe2O4 material prepared by coprecipitation. Nanosystems: physics, chemistry, mathematics, 2016, 7(3), P. 459–463.Nguyen A.T., Phan Ph.H.Nh.,Mittova I.Ya., Knurova M.V., Mittova V.O. The characterization of nanosized ZnFe2O4 material prepared by coprecipitation. Nanosystems: physics, chemistry, mathematics, 2016, 7(3), P. 459–463.Markov V.F. Hydrochemical deposition of metal sulphide films: modeling and experiment. Ekaterinburg, 2006, 217 p.Markov V.F. Hydrochemical deposition of metal sulphide films: modeling and experiment. Ekaterinburg, 2006, 217 p.Senik B.N. Application of crystals in promising developments of hyperspectral optical systems. Scientific and Technical Journal. Applied Physics, 2007, 3, P. 134–141.Senik B.N. Application of crystals in promising developments of hyperspectral optical systems. Scientific and Technical Journal. Applied Physics, 2007, 3, P. 134–141.Ksenevich V.K., Gorbachuk N.I., Viet Ho, Shuba M.V., Kuzhir P.P., Maksimenko S.A., Paddubskaya A.G., Valusis G., Wieck A.D., Zak A., Tenne R. Electrical properties of carbon nanotubes / WS2 nanotubes (nanoparticles) hybrid films. Nanosystems: physics, chemistry, mathematics, 2016, 7(1), P. 37–43.Ksenevich V.K., Gorbachuk N.I., Viet Ho, Shuba M.V., Kuzhir P.P., Maksimenko S.A., Paddubskaya A.G., Valusis G., Wieck A.D., Zak A., Tenne R. Electrical properties of carbon nanotubes / WS2 nanotubes (nanoparticles) hybrid films. Nanosystems: physics, chemistry, mathematics, 2016, 7(1), P. 37–43.Naumov A.V., Semenov V.N., Auerbach .. Thiourea coordination compounds in the synthesis of metal sulphide. Chemical industry, 2003, 80(2), P. 17–26.Naumov A.V., Semenov V.N., Auerbach .. Thiourea coordination compounds in the synthesis of metal sulphide. Chemical industry, 2003, 80(2), P. 17–26.Levin M.N., Semenov V.N., Ostapenko O.V. Photoelectric converters on heterostructures CdxZn1−xS/Cu2S. Applied Physics Letters, 2002, 28(10), P. 19–23.Levin M.N., Semenov V.N., Ostapenko O.V. Photoelectric converters on heterostructures CdxZn1−xS/Cu2S. Applied Physics Letters, 2002, 28(10), P. 19–23.Samofalova T.V., Ovechkina N.M., Lukin A.N., Semenov V.N. Structure and properties of lead sulphide films deposited from thiourea fusion compounds. Bulletin of the Technological University, 2012, 15(16), P. 68–70.Samofalova T.V., Ovechkina N.M., Lukin A.N., Semenov V.N. Structure and properties of lead sulphide films deposited from thiourea fusion compounds. Bulletin of the Technological University, 2012, 15(16), P. 68–70.Samofalova T.V., Ovechkina N.M., Kharin A.N., Semenov V.N. Surface microstructure of pyrolytic lead sulphide films. Condensed matter and interphases, 2013, 15(3), P. 332–336.Samofalova T.V., Ovechkina N.M., Kharin A.N., Semenov V.N. Surface microstructure of pyrolytic lead sulphide films. Condensed matter and interphases, 2013, 15(3), P. 332–336.Fedjukin A.V., Nituta A.N., Lukin A.N., Semenov V.N., Ovechkina N.M. Optical properties and structure of PbS films obtained by pyrolysis of thiourea complexes. Bulletin of the Russian Academy of Sciences. Physics, 2015, 79(2), P. 238–240.Fedjukin A.V., Nituta A.N., Lukin A.N., Semenov V.N., Ovechkina N.M. Optical properties and structure of PbS films obtained by pyrolysis of thiourea complexes. Bulletin of the Russian Academy of Sciences. Physics, 2015, 79(2), P. 238–240.

The authors declare that there are no conflicts of interest present.