<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE article PUBLIC "-//NLM//DTD JATS (Z39.96) Journal Publishing DTD v1.3 20210610//EN" "JATS-journalpublishing1-3.dtd">
<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="en"><front><journal-meta><journal-id journal-id-type="publisher-id">najo</journal-id><journal-title-group><journal-title xml:lang="en">Nanosystems: Physics, Chemistry, Mathematics</journal-title><trans-title-group xml:lang="ru"><trans-title>Наносистемы: физика, химия, математика</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">2220-8054</issn><issn pub-type="epub">2305-7971</issn><publisher><publisher-name>Университет ИТМО</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.17586/2220-8054-2018-9-4-532-536</article-id><article-id custom-type="elpub" pub-id-type="custom">najo-767</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>CHEMISTRY AND MATERIAL SCIENCE</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ХИМИЯ И МАТЕРИАЛОВЕДЕНИЕ</subject></subj-group></article-categories><title-group><article-title>Laboratory facility for working with supercritical fluids</article-title><trans-title-group xml:lang="ru"><trans-title></trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Izotov</surname><given-names>A. I.</given-names></name></name-alternatives><bio xml:lang="en"><p>R. Luxembourg str. 72, 83114</p><p>Donetsk</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Kilman</surname><given-names>G. V.</given-names></name></name-alternatives><bio xml:lang="en"><p>R. Luxembourg str. 72, 83114</p><p>Donetsk</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Shalaev</surname><given-names>R. V.</given-names></name></name-alternatives><bio xml:lang="en"><p>R. Luxembourg str. 72, 83114</p><p>Donetsk</p></bio><email xlink:type="simple">sharos@donfti.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="western" xml:lang="en"><surname>Prudnikov</surname><given-names>A. M.</given-names></name></name-alternatives><bio xml:lang="en"><p>R. Luxembourg str. 72, 83114</p><p>Donetsk</p></bio><xref ref-type="aff" rid="aff-1"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="en">Donetsk Institute for Physics and Engineering named after A. A. Galkin<country>Ukraine</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2018</year></pub-date><pub-date pub-type="epub"><day>13</day><month>08</month><year>2025</year></pub-date><volume>9</volume><issue>4</issue><fpage>532</fpage><lpage>536</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Izotov A.I., Kilman G.V., Shalaev R.V., Prudnikov A.M., 2025</copyright-statement><copyright-year>2025</copyright-year><copyright-holder xml:lang="ru">Izotov A.I., Kilman G.V., Shalaev R.V., Prudnikov A.M.</copyright-holder><copyright-holder xml:lang="en">Izotov A.I., Kilman G.V., Shalaev R.V., Prudnikov A.M.</copyright-holder><license license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://nanojournal.ifmo.ru/jour/article/view/767">https://nanojournal.ifmo.ru/jour/article/view/767</self-uri><abstract><p>An apparatus for working with supercritical fluids has been developed, and results have been obtained on purification of the diamond blend by supercritical isopropanol, as well as by selective etching of CNx films. It is shown that the proposed method for purifying diamond blend in supercritical isopropanol is not only effective, but also quite simple to use.</p></abstract><kwd-group xml:lang="en"><kwd>supercritical fluids</kwd><kwd>diamond blend</kwd><kwd>carbon nitride</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Beketova A.B., Kasenova Zh.M. State of the art of progress Supercritical fluid technologies. Bulletin of the L. N. Gumilyov Eurasian National University, 2012, 4, P. 249–255.</mixed-citation><mixed-citation xml:lang="en">Beketova A.B., Kasenova Zh.M. State of the art of progress Supercritical fluid technologies. Bulletin of the L. N. Gumilyov Eurasian National University, 2012, 4, P. 249–255.</mixed-citation></citation-alternatives></ref><ref id="cit2"><label>2</label><citation-alternatives><mixed-citation xml:lang="ru">Zalepugin D.Yu., Tilkunova N.., Chernyshova I.V., Polyakov V.S. Development of technologies based on supercritical fluids. Supercritical fluids: theory and practice, 2006, 1 (1), P. 27–51.</mixed-citation><mixed-citation xml:lang="en">Zalepugin D.Yu., Tilkunova N.., Chernyshova I.V., Polyakov V.S. Development of technologies based on supercritical fluids. Supercritical fluids: theory and practice, 2006, 1 (1), P. 27–51.</mixed-citation></citation-alternatives></ref><ref id="cit3"><label>3</label><citation-alternatives><mixed-citation xml:lang="ru">Buslaeva E.Yu., Gubin S.P. Supercritical isopropanol as a reducing agent for inorganic oxides. Supercritical fluids: theory and practice, 2009, 4 (4), P. 73–96.</mixed-citation><mixed-citation xml:lang="en">Buslaeva E.Yu., Gubin S.P. Supercritical isopropanol as a reducing agent for inorganic oxides. Supercritical fluids: theory and practice, 2009, 4 (4), P. 73–96.</mixed-citation></citation-alternatives></ref><ref id="cit4"><label>4</label><citation-alternatives><mixed-citation xml:lang="ru">Uglov V.V., Shimanski V.I., Rusalsky D.P., Samtsov M.P. Spectral analysis of the structure of ultradispersed diamonds. Journal of Applied Spectroscopy, 2008, 75 (4), P. 546–549.</mixed-citation><mixed-citation xml:lang="en">Uglov V.V., Shimanski V.I., Rusalsky D.P., Samtsov M.P. Spectral analysis of the structure of ultradispersed diamonds. Journal of Applied Spectroscopy, 2008, 75 (4), P. 546–549.</mixed-citation></citation-alternatives></ref><ref id="cit5"><label>5</label><citation-alternatives><mixed-citation xml:lang="ru">Baidakova M.V., Kukushkina Yu.A., Sitnikova A.A., Yagovkina M.A. et al. Structure of nanodiamonds prepared by laser synthesis. Physics of the Solid State, 2013, 55 (8), P. 1747–1753.</mixed-citation><mixed-citation xml:lang="en">Baidakova M.V., Kukushkina Yu.A., Sitnikova A.A., Yagovkina M.A. et al. Structure of nanodiamonds prepared by laser synthesis. Physics of the Solid State, 2013, 55 (8), P. 1747–1753.</mixed-citation></citation-alternatives></ref><ref id="cit6"><label>6</label><citation-alternatives><mixed-citation xml:lang="ru">Ferrari A.C., Robertson J. Origin of the 1150 cm−1 Raman mode in nanocrystalline diamond. Phys. Rev. B, 2001, 63 (12), P. 121405-4.</mixed-citation><mixed-citation xml:lang="en">Ferrari A.C., Robertson J. Origin of the 1150 cm−1 Raman mode in nanocrystalline diamond. Phys. Rev. B, 2001, 63 (12), P. 121405-4.</mixed-citation></citation-alternatives></ref><ref id="cit7"><label>7</label><citation-alternatives><mixed-citation xml:lang="ru">Robertson J., OReilly E.P. Electronic and atomic structure of amorphous carbon. Phys. Rev. B, 1987, 35, P. 2946–2957.</mixed-citation><mixed-citation xml:lang="en">Robertson J., OReilly E.P. Electronic and atomic structure of amorphous carbon. Phys. Rev. B, 1987, 35, P. 2946–2957.</mixed-citation></citation-alternatives></ref><ref id="cit8"><label>8</label><citation-alternatives><mixed-citation xml:lang="ru">Kolpakov A.Ya., Sujanskaya I.V., Galkina M.E., et al. Effect of the degree of nitrogen doping and thickness on the electrical conductivity and morphology of nanoscale carbon coatings on silicon. Russian nanotechnology, 2011, 6 (3-4), P. 43–45.</mixed-citation><mixed-citation xml:lang="en">Kolpakov A.Ya., Sujanskaya I.V., Galkina M.E., et al. Effect of the degree of nitrogen doping and thickness on the electrical conductivity and morphology of nanoscale carbon coatings on silicon. Russian nanotechnology, 2011, 6 (3-4), P. 43–45.</mixed-citation></citation-alternatives></ref><ref id="cit9"><label>9</label><citation-alternatives><mixed-citation xml:lang="ru">Dolmatov V.Yu. Detonation-synthesis nanodiamonds: synthesis, structure, properties and applications. Russ. Chem. Rev., 2007, 76 (4), P. 339–360.</mixed-citation><mixed-citation xml:lang="en">Dolmatov V.Yu. Detonation-synthesis nanodiamonds: synthesis, structure, properties and applications. Russ. Chem. Rev., 2007, 76 (4), P. 339–360.</mixed-citation></citation-alternatives></ref><ref id="cit10"><label>10</label><citation-alternatives><mixed-citation xml:lang="ru">Sushchev V.G., Dolmatov V.Yu., Marchukov V.A., and Veretennikova M.V. Principles of the chemical purification of detonation diamondcontaining mixture by nitric acid. Journal of Superhard Materials, 2008, 5, P. 16–25.</mixed-citation><mixed-citation xml:lang="en">Sushchev V.G., Dolmatov V.Yu., Marchukov V.A., and Veretennikova M.V. Principles of the chemical purification of detonation diamondcontaining mixture by nitric acid. Journal of Superhard Materials, 2008, 5, P. 16–25.</mixed-citation></citation-alternatives></ref></ref-list><fn-group><fn fn-type="conflict"><p>The authors declare that there are no conflicts of interest present.</p></fn></fn-group></back></article>
