najoNanosystems: Physics, Chemistry, MathematicsНаносистемы: физика, химия, математика2220-80542305-7971Университет ИТМО10.17586/2220-8054-2016-7-1-140-145najo-825Research ArticlePAPERS, PRESENTED AT THE CONFERENCEPAPERS, PRESENTED AT THE CONFERENCEExpress analysis of endohedral fullerenes amount contained at fullerene mixtureExpress analysis of endohedral fullerenes amount contained at fullerene mixtureChurilovG. N.ChurilovG. N.

Krasnoyarsk

Krasnoyarsk

churilov@iph.krasn.ruPopovA. A.PopovA. A.

Dresden

Dresden

GuliaevaU. E.GuliaevaU. E.

Krasnoyarsk

Krasnoyarsk

SamoylovaN. A.SamoylovaN. A.

Dresden

Dresden

VnukovaN. G.VnukovaN. G.

Krasnoyarsk

Krasnoyarsk

KolonenkoA. L.KolonenkoA. L.

Krasnoyarsk

Krasnoyarsk

IsakovaV. G.IsakovaV. G.

Krasnoyarsk

Krasnoyarsk

DudnikA. I.DudnikA. I.

Krasnoyarsk

Krasnoyarsk

KoravanetsV. S.KoravanetsV. S.

Krasnoyarsk

Krasnoyarsk

Kirensky Institute of Physic SB RAS; Siberian Federal UniversityKirensky Institute of Physic SB RAS; Siberian Federal UniversityLeibniz Institute for Solid State and Materials ResearchLeibniz Institute for Solid State and Materials ResearchKirensky Institute of Physic SB RASKirensky Institute of Physic SB RASSiberian Federal UniversitySiberian Federal University20161408202571Special Issue: Proceedings of the 12th Biennial International Conference “Advanced Carbon Nanostructures” (ACNS’2015)140145Copyright © Churilov G.N., Popov A.A., Guliaeva U.E., Samoylova N.A., Vnukova N.G., Kolonenko A.L., Isakova V.G., Dudnik A.I., Koravanets V.S., 20252025Churilov G.N., Popov A.A., Guliaeva U.E., Samoylova N.A., Vnukova N.G., Kolonenko A.L., Isakova V.G., Dudnik A.I., Koravanets V.S.Churilov G.N., Popov A.A., Guliaeva U.E., Samoylova N.A., Vnukova N.G., Kolonenko A.L., Isakova V.G., Dudnik A.I., Koravanets V.S.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://nanojournal.ifmo.ru/jour/article/view/825

This paper describes the technique for rapid determination of endohedral metallofullerene (EMF) content in a fullerene mixture (FM). The methods of mass spectroscopy and atom emission element analysis underlay at the technique. By the method of mass spectroscopy, the type of EMF with atom-guest is registered and by the method of emission spectroscopy, the quantity of that element which is contained in the FM is determined. The technique may be used for rapid determination of EMF weight percents in the FM in the specific case if only one type of EMF is present, and of EMF average content if there are different types of EMF are present. The technique is demonstrated through the example of analysis of FM with Y, which was extracted from the carbon condensate (CC) by different solvents (C5H5N and CS2).

This paper describes the technique for rapid determination of endohedral metallofullerene (EMF) content in a fullerene mixture (FM). The methods of mass spectroscopy and atom emission element analysis underlay at the technique. By the method of mass spectroscopy, the type of EMF with atom-guest is registered and by the method of emission spectroscopy, the quantity of that element which is contained in the FM is determined. The technique may be used for rapid determination of EMF weight percents in the FM in the specific case if only one type of EMF is present, and of EMF average content if there are different types of EMF are present. The technique is demonstrated through the example of analysis of FM with Y, which was extracted from the carbon condensate (CC) by different solvents (C5H5N and CS2).

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The authors declare that there are no conflicts of interest present.