najoNanosystems: Physics, Chemistry, MathematicsНаносистемы: физика, химия, математика2220-80542305-7971Университет ИТМОnajo-895Research ArticleCHEMISTRY AND MATERIALS SCIENCEХИМИЯ И НАУКА О МАТЕРИАЛАХSynthesis and identification water-soluble tris-malonate of light fullerene – C60[=C(COOH)2]3SemenovK. N.

Saint-Petersburg

CharykovN. A.

Saint-Petersburg

KritchenkovA. S.

Saint-Petersburg

CherepkovaI. A.

Saint-Petersburg

ManyakinaO. S.

Saint-Petersburg

TyurinD. P.

Saint-Petersburg

ShestopalovaA. A.

Saint-Petersburg

KeskinovV. A.

Saint-Petersburg

keskinov@mail.ruIvanovaK. V.

Saint-Petersburg

IvanovaN. M.

Saint-Petersburg

LetenkoD. G.

Saint-Petersburg

NikitinV. A.

Saint-Petersburg

FokinaE. L.

Saint-Petersburg

RakhimovaO. V.

Saint-Petersburg

St. Petersburg State UniversityRussian FederationSt. Petersburg State Technological Institute (Technical University); St. Petersburg State Electro-Technical University (LETI)Russian FederationSt. Petersburg State Technological Institute (Technical University)Russian FederationSt. Petersburg State University Architecture AcademyRussian FederationSt. Petersburg State Technical UniversityRussian FederationSt. Petersburg State Electro-Technical University (LETI)Russian Federation20141408202552315–319Copyright © Semenov K.N., Charykov N.A., Kritchenkov A.S., Cherepkova I.A., Manyakina O.S., Tyurin D.P., Shestopalova A.A., Keskinov V.A., Ivanova K.V., Ivanova N.M., Letenko D.G., Nikitin V.A., Fokina E.L., Rakhimova O.V., 20252025Semenov K.N., Charykov N.A., Kritchenkov A.S., Cherepkova I.A., Manyakina O.S., Tyurin D.P., Shestopalova A.A., Keskinov V.A., Ivanova K.V., Ivanova N.M., Letenko D.G., Nikitin V.A., Fokina E.L., Rakhimova O.V.Semenov K.N., Charykov N.A., Kritchenkov A.S., Cherepkova I.A., Manyakina O.S., Tyurin D.P., Shestopalova A.A., Keskinov V.A., Ivanova K.V., Ivanova N.M., Letenko D.G., Nikitin V.A., Fokina E.L., Rakhimova O.V.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://nanojournal.ifmo.ru/jour/article/view/895

The water soluble tris-malonate adduct of light fullerene – C60[=C(COOH)2]3 was produced in laboratory quantities. The product was identified by several analytical methods: elementary H–C–O–N analysis, IR-, Electronic, NMR- Spectroscopy, Mass Spectrometry.

tris-malonate of light fullerenesynthesiselementary analysisIR-ElectronicNMR- SpectroscopyMass SpectrometryResearch was executed with the help of the equipment of the Resource Center ‘GeoModel’ of Saint-Petersburg State University. This work has been accomplished as the part of the Ministry of Education and Science of the Russian Federation research assignment ‘Realization of scientific research (fundamental studies, applied research and advanced developments)’. Project code: 2548.ReferencesLamparth I., Hirsch A. Water-soluble malonic acid derivatives of C60 with a defined three-dimensional structure. J. Chem. Soc. Chem. Commun., P. 1727–1728 (1994).Lamparth I., Hirsch A. Water-soluble malonic acid derivatives of C60 with a defined three-dimensional structure. J. Chem. Soc. Chem. Commun., P. 1727–1728 (1994).Semenov K.N., Charykov N.A., Pronskih A.E, Keskinov V.A. Fullerenol-70-d: synthesis, identification, polythermal solubility and density of water solutions. Nanosystems: Physics, Chemistry, Mathematics, 3 (6), . 1–10 (2012).Semenov K.N., Charykov N.A., Pronskih A.E, Keskinov V.A. Fullerenol-70-d: synthesis, identification, polythermal solubility and density of water solutions. Nanosystems: Physics, Chemistry, Mathematics, 3 (6), . 1–10 (2012).Semenov K.N., Charykov N.A., Keskinov V.A. Synthesis and Identification. Properties of Fullerenol Water Solutions. J. Chem. Eng. Data, 56, P. 230–239 (2011).Semenov K.N., Charykov N.A., Keskinov V.A. Synthesis and Identification. Properties of Fullerenol Water Solutions. J. Chem. Eng. Data, 56, P. 230–239 (2011).Semenov K.N., Charykov N.A. Solubility of Light Fullerenes and Fullerenol in Biocompatible with Human Beings Solvents. Chapter in Handbook: Grapes: Cultivation, Varieties and Nutritional Uses, Nova Sciences Publishers, Inc., Editor R.P. Murphy et al., P. 1–48 (2011).Semenov K.N., Charykov N.A. Solubility of Light Fullerenes and Fullerenol in Biocompatible with Human Beings Solvents. Chapter in Handbook: Grapes: Cultivation, Varieties and Nutritional Uses, Nova Sciences Publishers, Inc., Editor R.P. Murphy et al., P. 1–48 (2011).Semenov K.N., Charykov N.A. Phase Equilibria in the Fullerene-Containing Systems. Handbook on Fullerene: Synthesis, Properties and Applications. Editor R.F.Verner, C.Benvegny, P. 1–91 (2012).Semenov K.N., Charykov N.A. Phase Equilibria in the Fullerene-Containing Systems. Handbook on Fullerene: Synthesis, Properties and Applications. Editor R.F.Verner, C.Benvegny, P. 1–91 (2012).

The authors declare that there are no conflicts of interest present.