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Наносистемы: физика, химия, математика

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Synthesis and characterization of highly ordered nanosized PbS thin films: modified silar

https://doi.org/10.17586/2220-8054-2016-7-3-499-501

Аннотация

In the current status, we have successfully synthesized lead sulfide (PbS) thin films using a modified successive ionic layer absorption and reaction (SILAR) method. The synthesized film was characterized using UV-Vis-NIR spectrophotometer, X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM) techniques for optical, structural and morphological properties. Opto-structural study demonstrates that synthesized thin film has a pure crystal structure. The surface morphology study indicates a nanospherical surface morphology without pinhole on the substrate surfaces. Overall study clearly demonstrates that the synthesized PbS thin film by SILAR method have great potential for sensitization of oxide microstructure.

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Об авторах

Kishorkumar V. Khot
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Vishvanth B. Ghanwat
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Pallavi B. Patil
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Chaitali S. Bagade
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Rahul М. Mane
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Dadaso В. Shinde
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Sandip K. Jagadale
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Ji-hyung Jang
Nanocrystal Laboratory, School of Energy and Chemical engineering, Ulsan National Institute of Science and Technology (UNIST)
Южная Корея


P. N. Bhosale
Materials Research Laboratory, Department of Chemistry, Shivaji University
Индия

Kolhapur



Список литературы

1. Mondal A., Mukherjee N. Cubic PbS thin films on TCO glass substrate by galvanic technique. Mater. Lett., 2006, 60, P. 2672–2674.

2. Jauregui J.J.V., Bon R.R., Galvan A.M., Lerma M.S. Optical properties of PbS thin films chemically deposited at different temperatures. Thin Solid Films, 2003, 441, P. 104–110.

3. Khot K.V., Mali S.S., Mane R.M., Patil P.S., Hong C.K., Kim J.H., Heo J., Bhosale P.N. Synthesis, characterization and photoelectrochemical properties of PbS sensitized vertically aligned ZnO nanorods: Modified aqueous route. J Mater Sci: Mater Electron, 2015, 26, P. 6897–6906.

4. Saikia D., Phukan P. Fabrication and evaluation of CdS/PbS thin film solar cell by chemical bath deposition technique. Thin Solid Films, 2014, 562, P. 239.

5. Khot K.V., Mali S.S., Ghanwat V.B., Kharade S.D., Mane R.M., Hong C.K., Bhosale P.N. Photocurrent enhancement in a Cu2Cd(SSe)2 photoanode synthesized via an arrested precipitation route. New. J. Chem., 2016, 40, P. 3277.

6. Tohidi T., Ghaleh K.J., Namdar A., Ghaleh R.A. Comparative studies on the structural, morphological, optical, and electrical properties of nanocrystalline PbS thin films grown by chemical bath deposition using two different bath compositions. Mater. Sci.: Semicond. Process, 2014, 25, P. 197–206.

7. Khot K.V., Mali S.S., Pawar N.B., Mane R.M., Kondalkar V.V., Ghanwat V.B., Patil P.S., Hong C.K., Kim J.H., He J.o, Bhosale P.N. Novel synthesis of interconnected nanocubic PbS thin films by facile aqueous chemical route. J. Mater. Sci.: Mater. Electron, 2014, 25, P. 3762–3770.


Рецензия

Для цитирования:


Khot K.V., Ghanwat V.B., Patil P.B., Bagade Ch.S., Mane R.М., Shinde D.В., Jagadale S.K., Jang J., Bhosale P.N. Synthesis and characterization of highly ordered nanosized PbS thin films: modified silar. Наносистемы: физика, химия, математика. 2016;7(3):499-501. https://doi.org/10.17586/2220-8054-2016-7-3-499-501

For citation:


Khot K.V., Ghanwat V.B., Patil P.B., Bagade Ch.S., Mane R.M., Shinde D.B., Jagadale S.K., Jang J., Bhosale P.N. Synthesis and characterization of highly ordered nanosized PbS thin films: modified silar. Nanosystems: Physics, Chemistry, Mathematics. 2016;7(3):499-501. https://doi.org/10.17586/2220-8054-2016-7-3-499-501

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ISSN 2220-8054 (Print)
ISSN 2305-7971 (Online)