The characterization of nanosized ZnFe2O4 material prepared by coprecipitation
https://doi.org/10.17586/2220-8054-2016-7-3-459-463
Abstract
The nanosized ZnFe2O4 material was synthesized using the coprecipitation method from Zn2+ and Fe3+ cations in a boiling aqueous medium. The results of TG/DSC, XRD, SEM, TEM and VSM analysis show that the ZnFe2O4 material prepared after annealing at 600 ◦C had tetragonal structure, a size of 20 – 50 nm, Hc < 70 Oe, Mr < 0.5 emu/g and Ms ∼ 2.5 emu/g.
Supporting agencies: This work was supported by the Ministry of Education and Science of the Russian Federation in line with government order for Higher Education Institutions in the field of science for the years 2014 – 2016 (project No. 225)
About the Authors
A. T. Nguyen
Ho Chi Minh City Pedagogical University
Viet Nam
Viet Nam
Ho Chi Minh City
Ph. H. Nh. Phan
Ho Chi Minh City Pedagogical University
Viet Nam
Viet Nam
Ho Chi Minh City
I. Ya. Mittova
Voronezh State University
Viet Nam
Viet Nam
Voronezh
M. V. Knurova
Voronezh State University
Russian Federation
Russian Federation
Voronezh
V. O. Mittova
Voronezh State Medical University named after N.N. Burdenko
Russian Federation
Russian Federation
Voronezh
References
1. Luu T.T. Magnetic Materials Lecture. Hanoi National University Publication, 2008, 273 p.
2. Brusensov Yu.A., Minaev A.M. Fundamentals of physics and technology of oxide semiconductors. Publisher TSTU, Tambov, 2001, 40 p.
3. Al Angari Y.M. Magnetic properties of La-substituted NiFe2O4 via egg-white precursor route. Journal of Magnetism and Magnetic Materials, 2011, 323, P. 1835–1839.
4. Kuznetsova V.A., Almjasheva O.V., Gusarov V.V. Influence of microwave and ultrasonic treatment on the formation of CoFe2O4 under hydrothermal conditions. Glass Physics and Chemistry, 2009, 35(2), P. 205–209.
5. Komlev A.A., Semenova A.S. Magnetic Characteristics of MgFe2O4-containing nanopowders prepared by the hydrothermal method. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(6), P. 105–111. (In Russian)
6. Komlev A.A., Ilhan S. Formation of iron-magnesium spinel nanoparticles under dehydration of co-precipitated magnesium and iron hydroxides. Nanosystems: Physics, Chemistry, Mathematics, 2012, 3(4), P. 114–121. (In Russian)
7. Luu M.D., Nguyen Th.T.L. Synthesis nanosized CoFe2O4 by gel combustion. Vietnam Chemistry Journal, 2010, 48(4), P. 404–408.
8. Nguyen Th.T.L., Pham Th.H. Synthesis nanosized ZnMn2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(2), P. 174–179.
9. Nguyen A.T., Mittova I.Ya., et al. Influence of the preparation condition on the size and morphology of nanocrystalline lanthanum orthoferrite. Glass Physics and Chemistry, 2008, 34(6), P. 756–761.
10. Nguyen A.T., Mittova I.Ya., Almjasheva O.V. Influence of the synthesis conditions on the particle size and morphology of yttrium orthoferrite obtained from aqueous solutions. Russian Journal of Applied Chemistry, 2009, 82(11), P. 1915–1918.
11. Nguyen Th.T.L. Synthesis nanosized ZnFe2O4 by gel combustion. Vietnam Chemistry Journal, 2013, 51(3), P. 312–316.
12. Nazarenko V.A., Antonovich V.P., Nevskaya E.M. Metal ions hydrolysis in dilute solutions. Atomizdat, Moscow, 1979, 192 p.
Review
For citations:
Nguyen A.T., Phan P., Mittova I.Ya., Knurova M.V., Mittova V.O. The characterization of nanosized ZnFe2O4 material prepared by coprecipitation. Nanosystems: Physics, Chemistry, Mathematics. 2016;7(3):459-463. https://doi.org/10.17586/2220-8054-2016-7-3-459-463
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