Исследование физико-механических свойств и радиационной стойкости магний-индиевого феррита, синтезированного полимер-нитратным способом

В статье обсуждаются особенности полимер-нитратного синтеза высокодисперсных частиц магний-индиевого феррита (MgFeInO₄), и приводятся результаты экспериментального исследования физико-механических свойств керамики, изготовленной на их основе. По данным порошковой рентгеновской дифракции установлено, что однофазный порошок феррит-шпинели может быть получен только путем высокотемпературной обработки рентгеноаморфного прекурсора, образовавшегося в результате термического разложения смеси поливинилового спирта и нитратов металлов. Керамика, изготовленная с использованием субмикронных частиц MgFeInO₄, имеет плотность, близкую к теоретической. Из результатов измерения микротвердости по методу Виккерса установлено, что полученный материал обладает высокой твердостью. По данным спектроскопии диффузного отражения определено значение энергии ширины запрещенной зоны MgFeInO₄. С использованием кристаллографических и электрофизических характеристик синтезированного материала спрогнозирована его устойчивость к радиационно-индуцированным структурным изменениям.

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