The microstructure of the surface of thin PbS films deposited from the coordination compounds diacetatodi(thiourea)lead
https://doi.org/10.17586/2220-8054-2017-8-3-378-381
Abstract
This paper presents the results from a study of the microstructure of the surface of lead sulfide films deposited via the pyrolysis of aqueous [Pb(N2H4CS)2(CH3COO)2] aerosols. The influences of temperature and the concentration of thiourea on the synthesized films’ surface topography were investigated. A change in the type of conductivity with increasing temperature was observed.
Keywords
About the Authors
V. N. SemenovRussian Federation
Universitetskaya sq., 1, Voronezh 394018
A. N. Nituta
Russian Federation
Universitetskaya sq., 1, Voronezh 394018
A. N. Lukin
Russian Federation
Universitetskaya sq., 1, Voronezh 394018
N. M. Ovechkina
Russian Federation
Universitetskaya sq., 1, Voronezh 394018
L. N. Nikitin
Russian Federation
Universitetskaya sq., 1, Voronezh 394018
References
1. Kaupp G. Atomic force microscopy, scanning nearfield optical microscopy and nanoscratching. Application to rough and natural surfaces. Springer-Verlag, Berlin Heidelberg, 2006, 296 p.
2. Almjasheva O.V. Formation and structural transformations of nanoparticles in the TiO2–H2O system. Nanosystems: physics, chemistry, mathematics, 2016, 7(6), P. 1031–1049.
3. Nguyen A.T., Phan Ph.H.Nh.,Mittova I.Ya., Knurova M.V., Mittova V.O. The characterization of nanosized ZnFe2O4 material prepared by coprecipitation. Nanosystems: physics, chemistry, mathematics, 2016, 7(3), P. 459–463.
4. Markov V.F. Hydrochemical deposition of metal sulphide films: modeling and experiment. Ekaterinburg, 2006, 217 p.
5. Senik B.N. Application of crystals in promising developments of hyperspectral optical systems. Scientific and Technical Journal. Applied Physics, 2007, 3, P. 134–141.
6. Ksenevich V.K., Gorbachuk N.I., Viet Ho, Shuba M.V., Kuzhir P.P., Maksimenko S.A., Paddubskaya A.G., Valusis G., Wieck A.D., Zak A., Tenne R. Electrical properties of carbon nanotubes / WS2 nanotubes (nanoparticles) hybrid films. Nanosystems: physics, chemistry, mathematics, 2016, 7(1), P. 37–43.
7. Naumov A.V., Semenov V.N., Auerbach .. Thiourea coordination compounds in the synthesis of metal sulphide. Chemical industry, 2003, 80(2), P. 17–26.
8. Levin M.N., Semenov V.N., Ostapenko O.V. Photoelectric converters on heterostructures CdxZn1−xS/Cu2S. Applied Physics Letters, 2002, 28(10), P. 19–23.
9. Samofalova T.V., Ovechkina N.M., Lukin A.N., Semenov V.N. Structure and properties of lead sulphide films deposited from thiourea fusion compounds. Bulletin of the Technological University, 2012, 15(16), P. 68–70.
10. Samofalova T.V., Ovechkina N.M., Kharin A.N., Semenov V.N. Surface microstructure of pyrolytic lead sulphide films. Condensed matter and interphases, 2013, 15(3), P. 332–336.
11. Fedjukin A.V., Nituta A.N., Lukin A.N., Semenov V.N., Ovechkina N.M. Optical properties and structure of PbS films obtained by pyrolysis of thiourea complexes. Bulletin of the Russian Academy of Sciences. Physics, 2015, 79(2), P. 238–240.
Review
For citations:
Semenov V.N., Nituta A.N., Lukin A.N., Ovechkina N.M., Nikitin L.N. The microstructure of the surface of thin PbS films deposited from the coordination compounds diacetatodi(thiourea)lead. Nanosystems: Physics, Chemistry, Mathematics. 2017;8(3):378-381. https://doi.org/10.17586/2220-8054-2017-8-3-378-381