НАНОСИСТЕМЫ: ФИЗИКА, ХИМИЯ, МАТЕМАТИКА, 2010, ТОМ 1, № 1, С. 26–36
РАЗМЕР, МОРФОЛОГИЯ И СТРУКТУРА ЧАСТИЦ
НАНОПОРОШКА ДИОКСИДА ЦИРКОНИЯ,
ПОЛУЧЕННОГО В ГИДРОТЕРМАЛЬНЫХ УСЛОВИЯХ
О. В. Альмяшева(1), Б.А. Федоров(2), А.В. Смирнов(2), В. В. Гусаров(3),(4)
(1)Институт высокомолекулярных соединений РАН
(2)Санкт-Петербургский государственный университет информационных технологий,
механики и оптики
(3)Санкт-Петербургский государственный технологический институт (технический
университет)
(4)Физико-технический институт им. А.Ф. Иоффе РАН
victor.v.gusarov@gmail.com, almjasheva@mail.ru
С использованием методов просвечивающей электронной микроскопии, малоугловой и широкоугловой рентгеновской дифрактометрии, динамического рассеяния света, адсорбции и десорбции газов на поверхности определены морфологические и размерные параметры частиц нанопорошка ZrO2, синтезированного в гидротермальных условиях. Показано, что только совместный анализ результатов нескольких методов позволяет получить надежную информацию об этих параметрах наночастиц. На основании проведенного исследования полученных в гидротермальных условиях наночастиц ZrO2 они охарактеризованы овальной (близкой к округлой) формой, узким распределением частиц по размерам и средним размером около 12–18 нм.
Ключевые слова: наночастицы, нанопорошок, диоксид циркония, гидротермальный синтез, структура нанокристаллов, форма и размер наночастиц, электронная микроскопия, рассеяние рентгеновского излучения, динамическое рассеяние света.
УДК 54.06
PACS 61.46.+w; 81.07.-b
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