NANOSYSTEMS: PHYSICS, CHEMISTRY, MATHEMATICS, 2012, 3 (4), P. 101–113
MORPHOLOGY AND DIMENSIONAL PARAMETERS OF BOEHMITE NANOCRYSTALS OBTAINED UNDER HYDROTHERMAL CONDITIONS
Svetlana Kirillova – Saint Petersburg Electrotechnical University “LETI”, Saint Petersburg, Russia, assistant, refractory-sveta@mail.ru
Alexander Smirnov – Saint Petersburg National Research University of Information Technologies, Mechanics and Optics, Saint Petersburg, Russia, Associate Professor of Physics Department, Ph.D., smirnav@phd.ifmo.ru
Boris Fedorov – Saint Petersburg National Research University of Information Technologies, Mechanics and Optics, Saint Petersburg, Russia, Professor of Physics Department, Ph.D., borfedorov@rambler.ru
Andrey Krasilin – Ioffe Physical-Technical Institute RAS, Saint Petersburg, Russia, postgraduate, ikrasilin@gmail.com
Alexander Bugrov – Institute of Macromolecular Compounds, Saint Petersburg, Russia, postgraduate, bugrov.an@mail.ru
Kamil Gareev – Saint Petersburg Electrotechnical University “LETI”, Saint Petersburg, Russia, postgraduate, kggareev@yandex.ru
Irina Gracheva – Saint Petersburg Electrotechnical University “LETI”, Saint Petersburg, Russia, Associate professor, PhD, iegrachova@mail.ru
Vyacheslav Almjashev – Saint Petersburg Electrotechnical University “LETI”, Saint Petersburg, Russia, assistant, vac@mail.ru
The complex physicochemical investigation of the morphological parameters of boehmite nanoparticles and their agglomerates has been carried out. It is shown that a complex approach to the nanoparticle analysis can resolve the contradictions and to increase the reliability of measurement results. The possibilities of the method of small-angle X-ray scattering for the characterization of nanoparticle with isometric shape have been demonstrated. The features of the dynamic light scattering method in the analysis of lamellar nanoparticles agglomerates are considered.
Keywords: boehmite, nanoparticles, hydrothermal synthesis, particle morphology, particle size, size distribution, agglomerates, atomic force microscopy, scanning electron microscopy, dynamic light scattering, X-ray diffractometry, small-angle X-ray scattering, adsorption-desorption gas analysis (BET method).
UDC 544.08
The subsequent time I learn a blog, I hope that it doesnt disappoint me as a lot as this one. I mean, I do know it was my choice to learn, but I truly thought youd have something fascinating to say. All I hear is a bunch of whining about something that you possibly can fix if you werent too busy searching for attention.
As a Newbie, I am constantly exploring online for articles that can benefit me. Thank you
Can I just say what a relief to find someone who actually knows what theyre talking about on the internet. You definitely know how to bring an issue to light and make it important. More people need to read this and understand this side of the story. I cant believe youre not more popular because you definitely have the gift.