NANOSYSTEMS: PHYSICS, CHEMISTRY, MATHEMATICS, 2012, 3 (4), P. 114–121
FORMATION OF IRON-MAGNESIUM NANOPARTICLES UNDER DEHYDRATION OF COPRECIPITATED MAGNESIUM AND IRON HYDROXIDES
А. А. Komlev – Saint Petersburg State Institute of Technology (Technical University), Saint Petersburg, Russia, brain86@bk.ru
S. Ilhan – Metallurgical and Materials Engineering Department, Engineering Faculty, Istanbul University, Istanbul, Turkey, ilhans@istanbul.edu.tr
Formation mechanism of oxidic nanoparticles under dehydration of coprecipitated magnesium and iron hydroxides was studied. It was shown that magnesium-iron spinel starts to form at T=400°С and Р=500 atm. Depending on the phase formation size of spinel nanoparticles crystallites varies in range 4090 nm.
Keywords: hydrothermal synthesis, spinel, magnesium and iron layered double hydroxides, nanoparticles, non-autonomous phase, non-autonomous state of matter, X-ray analysis.
UDC 536.42
PACS 81.07.Wx
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