NANOSYSTEMS: PHYSICS, CHEMISTRY, MATHEMATICS, 2016, 7 (4), P. 765–767
Surfactant assisted synthesis of nanocrystalline n-Bi2Se3 thin films at room temperature via arrested precipitation technique
N. D. Desai – Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur–416004, India
S. M. Patil – Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur–416004, India
K.V. Khot – Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur–416004, India
R. M. Mane – Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur–416004, India
P. N. Bhosale – Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur–416004, India; p_n_bhosale@rediffmail.com
In the present investigation, we have successfully synthesized nanocrystalline bismuth selenide (Bi2Se3) thin films using an arrested precipitation technique at room temperature. The optostructural, morphological, compositional and photoeletrochemical properties were studied for Bi2Se3 thin films prepared via surfactant-assisted synthesis. The optical study reveals the presence of direct allowed transition with band gap energy ranging from 1.40–1.80 eV. The X-ray diffraction (XRD) pattern confirms rhombohedral crystal structure. Scanning electron microscopy study shows the morphological transition from an interconnected mesh to nanosphere-like morphology and finally, lamellar sphere. Atomic force microscopy (AFM) study carried out to determine surface roughness and surface topography of thin films. Energy dispersive spectroscopy (EDS) analysis reveals the presence and ratio of elemental bismuth and selenium. Finally, the photoelectrochemical (PEC) performance of all the as-synthesized thin films were carried out using iodidepolyiodide redox couple.
Keywords: Bi2Se3, APT, surfactant.
PACS 81.07.-b
DOI 10.17586/2220-8054-2016-7-4-765-767
Hello, Neat post. There’s a problem together with your web site in internet explorer, might check this… IE nonetheless is the marketplace chief and a huge portion of other people will omit your magnificent writing due to this problem.
Hey there! I’ve been following your site for some time now and finally got the bravery to go ahead and give you a shout out from Houston Tx! Just wanted to tell you keep up the fantastic work!
Nice post. I learn something more challenging on different blogs everyday. It will always be stimulating to read content from other writers and practice a little something from their store. I’d prefer to use some with the content on my blog whether you don’t mind. Natually I’ll give you a link on your web blog. Thanks for sharing.
I¦ve read a few good stuff here. Certainly price bookmarking for revisiting. I surprise how much attempt you put to make this sort of wonderful informative web site.
Thanks, I’ve recently been looking for information approximately this topic for a long time and yours is the best I’ve discovered so far. But, what concerning the bottom line? Are you certain in regards to the source?
But wanna input that you have a very nice internet site, I like the style and design it actually stands out.
AlphaBites Male is a dietary supplement designed to support men’s health, especially in areas related to energy, stamina, libido, and overall vitality.
FemiPro is a dietary supplement tailored specifically for women’s health, focusing on hormonal balance, energy, mood, and general well-being.
I’d should test with you here. Which isn’t something I often do! I get pleasure from studying a publish that may make folks think. Also, thanks for allowing me to comment!
I have been reading out some of your stories and i can claim pretty good stuff. I will definitely bookmark your blog.
Thank you for sharing excellent informations. Your site is very cool. I am impressed by the details that you have on this site. It reveals how nicely you understand this subject. Bookmarked this website page, will come back for more articles. You, my friend, ROCK! I found just the info I already searched everywhere and simply couldn’t come across. What a perfect web site.
Right now it sounds like WordPress is the best blogging platform available right now. (from what I’ve read) Is that what you are using on your blog?
Well I truly enjoyed reading it. This subject procured by you is very constructive for good planning.
Aw, this was a very nice post. In concept I would like to put in writing like this additionally – taking time and precise effort to make a very good article… but what can I say… I procrastinate alot and certainly not seem to get one thing done.
Simply want to say your article is as surprising. The clearness in your post is simply spectacular and i could assume you’re an expert on this subject. Well with your permission let me to grab your RSS feed to keep up to date with forthcoming post. Thanks a million and please continue the gratifying work.
Very interesting info!Perfect just what I was looking for!
I’ve been browsing online greater than three hours nowadays, but I never discovered any fascinating article like yours. It?¦s beautiful worth sufficient for me. In my opinion, if all webmasters and bloggers made good content material as you did, the internet can be a lot more helpful than ever before.
I have been absent for some time, but now I remember why I used to love this blog. Thanks, I will try and check back more frequently. How frequently you update your website?
I am forever thought about this, regards for posting.
Magnificent web site. Lots of useful information here. I am sending it to several pals ans also sharing in delicious. And obviously, thanks for your sweat!
Real instructive and excellent body structure of written content, now that’s user friendly (:.
Cool blog! Is your theme custom made or did you download it from somewhere? A design like yours with a few simple adjustements would really make my blog jump out. Please let me know where you got your theme. Kudos
Thanks a lot for sharing this with all people you actually recognize what you’re talking about! Bookmarked. Please also talk over with my website =). We can have a link trade agreement among us!
You are a very bright individual!
Thanx for the effort, keep up the good work Great work, I am going to start a small Blog Engine course work using your site I hope you enjoy blogging with the popular BlogEngine.net.Thethoughts you express are really awesome. Hope you will right some more posts.
As soon as I detected this site I went on reddit to share some of the love with them.
Thank you for sharing superb informations. Your web site is so cool. I am impressed by the details that you have on this website. It reveals how nicely you understand this subject. Bookmarked this website page, will come back for more articles. You, my friend, ROCK! I found simply the information I already searched everywhere and simply couldn’t come across. What a great web-site.
I have recently started a website, the information you offer on this site has helped me tremendously. Thank you for all of your time & work.
When I originally commented I clicked the -Notify me when new comments are added- checkbox and now each time a comment is added I get four emails with the same comment. Is there any way you can remove me from that service? Thanks!
Regards for this howling post, I am glad I discovered this website on yahoo.
Hey! I know this is kind of off topic but I was wondering if you knew where I could get a captcha plugin for my comment form? I’m using the same blog platform as yours and I’m having trouble finding one? Thanks a lot!
I’ve been exploring for a little bit for any high-quality articles or blog posts on this kind of house . Exploring in Yahoo I finally stumbled upon this web site. Reading this info So i’m satisfied to exhibit that I’ve an incredibly good uncanny feeling I came upon exactly what I needed. I such a lot surely will make certain to do not omit this website and provides it a glance on a continuing basis.
Good info. Lucky me I reach on your website by accident, I bookmarked it.
My spouse and I absolutely love your blog and find almost all of your post’s to be precisely what I’m looking for. Does one offer guest writers to write content to suit your needs? I wouldn’t mind publishing a post or elaborating on a few of the subjects you write related to here. Again, awesome web site!
Wow, wonderful blog layout! How long have you been blogging for? you made blogging look easy. The overall look of your web site is fantastic, as well as the content!
F*ckin’ remarkable things here. I am very glad to see your post. Thanks a lot and i’m looking forward to contact you. Will you please drop me a e-mail?
Perfect work you have done, this website is really cool with wonderful information.
Hey there this is kinda of off topic but I was wanting to know if blogs use WYSIWYG editors or if you have to manually code with HTML. I’m starting a blog soon but have no coding skills so I wanted to get guidance from someone with experience. Any help would be greatly appreciated!
I like this website its a master peace ! Glad I discovered this on google .
I really appreciate this post. I have been looking everywhere for this! Thank goodness I found it on Bing. You’ve made my day! Thanks again
I am curious to find out what blog platform you have been working with? I’m experiencing some minor security issues with my latest website and I’d like to find something more risk-free. Do you have any recommendations?
Wow! This could be one particular of the most useful blogs We’ve ever arrive across on this subject. Basically Excellent. I’m also an expert in this topic therefore I can understand your hard work.
Its great as your other articles : D, appreciate it for posting. “As experience widens, one begins to see how much upon a level all human things are.” by Joseph Farrell.
I went over this website and I think you have a lot of excellent information, saved to my bookmarks (:.
What i do not realize is if truth be told how you’re no longer really much more neatly-favored than you may be now. You are very intelligent. You already know thus significantly when it comes to this subject, made me in my view believe it from so many numerous angles. Its like women and men don’t seem to be fascinated unless it is one thing to do with Woman gaga! Your individual stuffs great. Always deal with it up!
Aw, this was a really nice post. In idea I wish to put in writing like this moreover – taking time and actual effort to make an excellent article… however what can I say… I procrastinate alot and not at all seem to get something done.
Very interesting topic, regards for putting up.
The next time I read a blog, I hope that it doesnt disappoint me as much as this one. I mean, I know it was my choice to read, but I actually thought youd have something interesting to say. All I hear is a bunch of whining about something that you could fix if you werent too busy looking for attention.
Well I truly enjoyed reading it. This tip provided by you is very useful for proper planning.
Wonderful work! This is the type of information that should be shared around the net. Shame on the seek engines for now not positioning this post upper! Come on over and visit my site . Thanks =)
I like what you guys are up too. Such intelligent work and reporting! Carry on the excellent works guys I’ve incorporated you guys to my blogroll. I think it’ll improve the value of my website
.
As a Newbie, I am continuously browsing online for articles that can benefit me. Thank you
I am glad to be one of the visitors on this outstanding website (:, thankyou for posting.
I loved as much as you’ll receive carried out right here. The sketch is attractive, your authored material stylish. nonetheless, you command get got an edginess over that you wish be delivering the following. unwell unquestionably come further formerly again as exactly the same nearly very often inside case you shield this hike.
Perfect work you have done, this site is really cool with wonderful information.
I am glad for commenting to let you know what a amazing experience my daughter found reading through your web site. She learned too many things, with the inclusion of what it is like to have an incredible giving style to let other individuals just completely grasp a variety of specialized subject matter. You truly surpassed my expectations. Thanks for offering those informative, safe, educational and cool tips on your topic to Lizeth.
Hey there! I know this is kind of off topic but I was wondering which blog platform are you using for this website? I’m getting sick and tired of WordPress because I’ve had issues with hackers and I’m looking at alternatives for another platform. I would be fantastic if you could point me in the direction of a good platform.
Dead indited subject material, appreciate it for information .
Thank you for another informative web site. Where else could I get that type of info written in such a perfect way? I have a project that I am just now working on, and I have been on the look out for such info.
Greetings from Colorado! I’m bored to death at work so I decided to check out your blog on my iphone during lunch break. I love the knowledge you provide here and can’t wait to take a look when I get home. I’m amazed at how fast your blog loaded on my phone .. I’m not even using WIFI, just 3G .. Anyways, good blog!
I have recently started a web site, the information you offer on this site has helped me greatly. Thanks for all of your time & work. “The man who fights for his fellow-man is a better man than the one who fights for himself.” by Clarence Darrow.
There is visibly a lot to identify about this. I assume you made various good points in features also.
Merely wanna comment on few general things, The website pattern is perfect, the articles is real wonderful : D.
I was reading some of your articles on this site and I think this website is rattling instructive! Continue putting up.
Hey there! I could have sworn I’ve been to this blog before but after browsing through some of the post I realized it’s new to me. Nonetheless, I’m definitely delighted I found it and I’ll be bookmarking and checking back often!
Thankyou for this wondrous post, I am glad I noticed this site on yahoo.
Terrific work! This is the type of information that should be shared around the internet. Shame on the search engines for not positioning this post higher! Come on over and visit my site . Thanks =)
There is evidently a lot to realize about this. I consider you made some nice points in features also.
As I website owner I conceive the written content here is real superb, regards for your efforts.
Howdy! Quick question that’s totally off topic. Do you know how to make your site mobile friendly? My weblog looks weird when browsing from my iphone 4. I’m trying to find a template or plugin that might be able to fix this issue. If you have any recommendations, please share. Many thanks!
Heya i am for the first time here. I came across this board and I find It really useful & it helped me out a lot. I hope to give something back and help others like you helped me.
Great tremendous things here. I?¦m very satisfied to peer your post. Thank you so much and i’m having a look ahead to touch you. Will you please drop me a e-mail?
It is in point of fact a nice and useful piece of info. I am glad that you just shared this helpful info with us. Please stay us up to date like this. Thank you for sharing.
Whats Taking place i’m new to this, I stumbled upon this I’ve found It positively helpful and it has aided me out loads. I hope to contribute & assist different customers like its helped me. Great job.
Very interesting information!Perfect just what I was searching for! “Energy is the power that drives every human being. It is not lost by exertion by maintained by it.” by Germaine Greer.
I’ve read some excellent stuff here. Certainly worth bookmarking for revisiting. I surprise how a lot effort you set to make such a excellent informative website.
It’s laborious to search out knowledgeable folks on this subject, but you sound like you understand what you’re talking about! Thanks
It’s appropriate time to make some plans for the future and it’s time to be happy. I’ve read this post and if I could I desire to suggest you few interesting things or tips. Maybe you could write next articles referring to this article. I want to read even more things about it!
I genuinely enjoy examining on this website, it holds wonderful posts. “One should die proudly when it is no longer possible to live proudly.” by Friedrich Wilhelm Nietzsche.
I don’t commonly comment but I gotta say thanks for the post on this amazing one : D.
It’s perfect time to make some plans for the future and it is time to be happy. I’ve read this post and if I could I want to suggest you some interesting things or tips. Perhaps you can write next articles referring to this article. I want to read even more things about it!
I feel that is one of the so much significant info for me. And i’m satisfied reading your article. However should remark on some common things, The site style is wonderful, the articles is actually great : D. Good activity, cheers
Appreciating the time and effort you put into your site and in depth information you present. It’s nice to come across a blog every once in a while that isn’t the same old rehashed material. Excellent read! I’ve bookmarked your site and I’m including your RSS feeds to my Google account.
You should participate in a contest for one of the best blogs on the web. I’ll recommend this site!
Thanks for ones marvelous posting! I certainly enjoyed reading it, you are a great author.I will remember to bookmark your blog and will often come back sometime soon. I want to encourage you continue your great work, have a nice weekend!
Really great visual appeal on this website , I’d value it 10 10.
I am impressed with this website , really I am a fan.
The subsequent time I read a blog, I hope that it doesnt disappoint me as a lot as this one. I mean, I do know it was my option to read, but I truly thought youd have something interesting to say. All I hear is a bunch of whining about something that you can repair in the event you werent too busy in search of attention.
You are my aspiration, I have few web logs and very sporadically run out from to post .
Hi my loved one! I want to say that this post is amazing, nice written and come with almost all important infos. I would like to peer more posts like this .
I genuinely enjoy looking at on this site, it has superb content.
I have recently started a blog, the information you offer on this web site has helped me tremendously. Thank you for all of your time & work. “Quit worrying about your health. It’ll go away.” by Robert Orben.
Rattling clear internet site, regards for this post.
Hiya, I’m really glad I have found this info. Nowadays bloggers publish just about gossips and web and this is really irritating. A good blog with exciting content, that’s what I need. Thank you for keeping this web site, I’ll be visiting it. Do you do newsletters? Can’t find it.
Hey there! Someone in my Myspace group shared this site with us so I came to give it a look. I’m definitely loving the information. I’m bookmarking and will be tweeting this to my followers! Wonderful blog and great design and style.
I will right away grab your rss feed as I can’t find your e-mail subscription link or e-newsletter service. Do you’ve any? Kindly let me know in order that I could subscribe. Thanks.
Great goods from you, man. I have bear in mind your stuff previous to and you are simply extremely magnificent. I really like what you have got here, certainly like what you are stating and the way in which wherein you say it. You make it entertaining and you still care for to stay it sensible. I can’t wait to read far more from you. This is actually a great web site.
Thanks for every other wonderful article. Where else may anyone get that type of info in such an ideal means of writing? I’ve a presentation next week, and I’m at the look for such info.
I’ve been browsing on-line more than three hours today, but I never discovered any attention-grabbing article like yours. It is pretty price sufficient for me. In my view, if all web owners and bloggers made just right content material as you probably did, the web can be much more useful than ever before.
Thank you for the sensible critique. Me & my neighbor were just preparing to do some research on this. We got a grab a book from our area library but I think I learned more from this post. I’m very glad to see such excellent information being shared freely out there.
I like what you guys are up also. Such intelligent work and reporting! Keep up the excellent works guys I have incorporated you guys to my blogroll. I think it will improve the value of my website
Hey, you used to write excellent, but the last several posts have been kinda boringK I miss your super writings. Past several posts are just a little bit out of track! come on!
This web site is my intake, very good design and perfect content material.
I was looking at some of your posts on this site and I conceive this website is real informative! Retain putting up.
When I originally commented I clicked the -Notify me when new comments are added- checkbox and now each time a comment is added I get four emails with the same comment. Is there any way you can remove me from that service? Thanks!
you’re really a good webmaster. The web site loading speed is amazing. It seems that you are doing any unique trick. Also, The contents are masterpiece. you’ve done a wonderful job on this topic!
The next time I read a blog, I hope that it doesnt disappoint me as much as this one. I mean, I know it was my choice to read, but I actually thought youd have something interesting to say. All I hear is a bunch of whining about something that you could fix if you werent too busy looking for attention.
As I web-site possessor I believe the content material here is rattling excellent , appreciate it for your hard work. You should keep it up forever! Good Luck.
Thank you for another informative blog. Where else could I get that type of information written in such an ideal way? I have a project that I am just now working on, and I’ve been on the look out for such information.
You made some good points there. I looked on the internet for the issue and found most people will go along with with your blog.
Only wanna remark on few general things, The website layout is perfect, the content is real great. “I delight in men over seventy. They always offer one the devotion of a lifetime.” by Oscar Fingall O’Flahertie Wills Wilde.
Whoa! This blog looks just like my old one! It’s on a completely different topic but it has pretty much the same layout and design. Superb choice of colors!
I like what you guys are up too. Such intelligent work and reporting! Carry on the excellent works guys I have incorporated you guys to my blogroll. I think it will improve the value of my web site
.
Its good as your other posts : D, thankyou for putting up. “There’s no Walter Cronkite to give you the final word each evening.” by William Weld.
ALPHA BITES
I like what you guys are up too. Such smart work and reporting! Carry on the superb works guys I¦ve incorporated you guys to my blogroll. I think it will improve the value of my web site
I’m really impressed with your writing skills as well as with the layout on your blog. Is this a paid theme or did you customize it yourself? Either way keep up the nice quality writing, it is rare to see a nice blog like this one these days..
Carbofire
You have brought up a very wonderful details, thanks for the post.
I really appreciate this post. I have been looking all over for this! Thank goodness I found it on Bing. You have made my day! Thanks again
I besides believe so , perfectly pent post! .
Just wish to say your article is as astonishing. The clearness in your post is simply cool and i can assume you are an expert on this subject. Well with your permission allow me to grab your feed to keep up to date with forthcoming post. Thanks a million and please keep up the enjoyable work.
Everything is very open and very clear explanation of issues. was truly information. Your website is very useful. Thanks for sharing.
I feel that is one of the most significant info for me. And i am happy studying your article. However should observation on few normal issues, The web site taste is wonderful, the articles is in point of fact great : D. Excellent process, cheers
Magnificent items from you, man. I’ve take note your stuff prior to and you’re just too great. I actually like what you’ve got here, certainly like what you’re saying and the way in which by which you assert it. You’re making it enjoyable and you continue to care for to keep it sensible. I cant wait to learn far more from you. That is actually a wonderful site.
Neuroquiet review
I think this site has some real wonderful information for everyone. “The individual will always be a minority. If a man is in a minority of one, we lock him up.” by Oliver Wendell Holmes.
Keep functioning ,terrific job!
Leanbiome
Thanks – Enjoyed this update, can you make it so I get an email every time you publish a new post?
I was more than happy to search out this internet-site.I wished to thanks in your time for this wonderful read!! I undoubtedly having fun with every little bit of it and I’ve you bookmarked to check out new stuff you weblog post.
When I originally commented I clicked the -Notify me when new comments are added- checkbox and now each time a comment is added I get four emails with the same comment. Is there any way you can remove me from that service? Thanks!
Alpha bites review
Herpesyl review
I really like your writing style, wonderful information, appreciate it for putting up
. “In university they don’t tell you that the greater part of the law is learning to tolerate fools.” by Doris Lessing.
Wonderful web site. A lot of useful info here. I am sending it to several friends ans also sharing in delicious. And obviously, thanks for your sweat!
Very interesting info !Perfect just what I was looking for!
I have read some good stuff here. Certainly price bookmarking for revisiting. I surprise how a lot attempt you set to create such a magnificent informative web site.
Gumaktiv
Tonic greens
Billionaire Brain Ware
I think you have mentioned some very interesting points, thanks for the post.
Kerassentials review
You have brought up a very great details, thankyou for the post.
Quietum plus review
Hey would you mind stating which blog platform you’re working with? I’m going to start my own blog soon but I’m having a difficult time deciding between BlogEngine/Wordpress/B2evolution and Drupal. The reason I ask is because your layout seems different then most blogs and I’m looking for something completely unique. P.S Apologies for being off-topic but I had to ask!
Hi! I just wanted to ask if you ever have any trouble with hackers? My last blog (wordpress) was hacked and I ended up losing many months of hard work due to no data backup. Do you have any solutions to stop hackers?
Mitolyn
Everything is very open and very clear explanation of issues. was truly information. Your website is very useful. Thanks for sharing.
Helpful info. Lucky me I discovered your web site by accident, and I am shocked why this twist of fate didn’t happened in advance! I bookmarked it.
Nagano Lean Body Tonic
Excellent goods from you, man. I’ve keep in mind your stuff prior to and you’re simply extremely excellent. I really like what you have got right here, certainly like what you are stating and the way in which wherein you say it. You are making it entertaining and you continue to care for to stay it sensible. I can not wait to learn far more from you. This is really a wonderful web site.
I envy your work, thanks for all the good posts.
You are a very smart person!
Lottery defeater software
I am continuously invstigating online for posts that can aid me. Thank you!
I truly enjoy studying on this web site, it holds superb posts. “It is easy to be nice, even to an enemy – from lack of character.” by Dag Hammarskjld.
I?¦ve recently started a web site, the info you offer on this site has helped me greatly. Thank you for all of your time & work.
THE MONEY WAVE REVIEW
Hiya, I am really glad I have found this info. Today bloggers publish just about gossips and net and this is actually irritating. A good website with exciting content, this is what I need. Thanks for keeping this web-site, I will be visiting it. Do you do newsletters? Can’t find it.
I simply needed to appreciate you once more. I do not know what I would’ve followed in the absence of the type of concepts shown by you concerning this concern. Completely was a real depressing condition for me personally, but being able to see the very well-written tactic you treated that forced me to cry with fulfillment. Now i am happier for your work and in addition expect you know what a great job you happen to be doing instructing other individuals all through your webblog. I am certain you’ve never encountered any of us.
Perfectly composed written content, thank you for selective information. “He who establishes his argument by noise and command shows that his reason is weak.” by Michel de Montaigne.
There’s noticeably a bundle to find out about this. I assume you made sure nice points in options also.
With havin so much content do you ever run into any issues of plagorism or copyright violation? My site has a lot of unique content I’ve either written myself or outsourced but it seems a lot of it is popping it up all over the web without my permission. Do you know any solutions to help protect against content from being ripped off? I’d really appreciate it.
Great post however I was wanting to know if you could write a litte more on this topic? I’d be very grateful if you could elaborate a little bit further. Appreciate it!
Thanks for sharing superb informations. Your web-site is very cool. I’m impressed by the details that you¦ve on this site. It reveals how nicely you perceive this subject. Bookmarked this website page, will come back for extra articles. You, my pal, ROCK! I found just the info I already searched everywhere and just could not come across. What a perfect site.
Whats Going down i’m new to this, I stumbled upon this I’ve found It positively helpful and it has helped me out loads. I hope to contribute & help different users like its aided me. Good job.
Very excellent information can be found on site.
I got what you intend,saved to fav, very decent website .
Good day! I know this is kind of off topic but I was wondering if you knew where I could get a captcha plugin for my comment form? I’m using the same blog platform as yours and I’m having problems finding one? Thanks a lot!
I discovered your blog site on google and check a few of your early posts. Continue to keep up the very good operate. I just additional up your RSS feed to my MSN News Reader. Seeking forward to reading more from you later on!…
Hello, i read your blog occasionally and i own a similar one and i was just curious if you get a lot of spam remarks? If so how do you prevent it, any plugin or anything you can advise? I get so much lately it’s driving me mad so any assistance is very much appreciated.